1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether

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Chemical Name:1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether
CAS No.:852866-26-3
Molecular Formula:C₃₆H₆₀O₁₂
Molecular Weight:684.865
Hs Code.:

Synonyms:1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether

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Chemical Property of 1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether

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Technology Process of 1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether

There total 2 articles about 1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2163-11-3
2-(2-tetrahydropyran-2-yloxyethanoxy)ethanol

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 852866-26-3
1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether

Guidance literature:: 2-(2-tetrahydropyran-2-yloxyethanoxy)ethanol; With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; at 20 ℃; for 1h;

1,3,5-Tris(bromomethyl)benzene; In tetrahydrofuran; for 3h; Heating;
DOI:10.1021/ja048655d

Reference yield:

: 54533-84-5
2-(2-(2-chloroethoxy)ethoxy)tetrahydro-2H-pyran

: 852866-26-3
1,3,5-tris(7'-hydroxy-2',5'-dioxa-1'-heptyl)benzene tri(2'-tetrahydropyranyl) ether

Guidance literature:: Multi-step reaction with 2 steps

1: NaI, NaHCO₃ / acetonitrile / 12 h / Heating

2: NaH / tetrahydrofuran / 72 h / Heating

With sodium hydride; sodium hydrogencarbonate; sodium iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00079a013