(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester

Base Information

Chemical Name:(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester
CAS No.:1258782-46-5
Molecular Formula:C₂₈H₄₀O₄
Molecular Weight:440.623
Hs Code.:

Synonyms:(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester

Chemical Property:

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Technology Process of (9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester

There total 2 articles about (9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 463-40-1,1955-33-5,21661-10-9,21661-09-6,21661-13-2,21661-11-0
(9Z,12Z,15Z)-octadeca-9-12,15-trienoic acid

: 1708-40-3
2-phenyl-[1,3]dioxan-5-ol

: 1258782-47-6,56554-38-2
(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester

: 1258782-46-5,56554-38-2
(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1016/j.tet.2010.09.070

Reference yield:

: 463-40-1,1955-33-5,21661-10-9,21661-09-6,21661-13-2,21661-11-0
(9Z,12Z,15Z)-octadeca-9-12,15-trienoic acid

: 100-52-7
benzaldehyde

: 56-81-5,25618-55-7,64333-26-2,8013-25-0
glycerol

: 1258782-47-6,56554-38-2
(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester

: 1258782-46-5,56554-38-2
(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester

: 56847-06-4
(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid trans-(2-phenyl-[1,3]dioxolan-4-yl)methyl ester

: 56847-06-4
(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-(2-phenyl-[1,3]dioxolan-4-yl)methyl ester

Guidance literature:: benzaldehyde; glycerol; Inert atmosphere;

(9Z,12Z,15Z)-octadeca-9-12,15-trienoic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tet.2010.09.070

Reference yield:

: 506-12-7
heptadecanoic acid

: 1258782-46-5,56554-38-2
(9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester

: 55268-58-1
(Z,Z,Z)-linolenic acid 2-hydroxy-1-(hydroxymethyl)ethyl ester

: 118605-13-3
C₂₀H₄₀O₄

Guidance literature:: heptadecanoic acid; (9Z,12Z,15Z)-octadeca-9,12,15-trienoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester; With trifluoroacetic anhydride; In dichloromethane; at 0 - 20 ℃; for 72h; Inert atmosphere;

With porcine pancreatin; water; sodium cholate; calcium chloride; at 40 ℃; pH=8; regioselective reaction; Inert atmosphere; aq. buffer; Enzymatic reaction;
DOI:10.1016/j.tet.2010.09.070