N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Base Information

Chemical Name:N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide
CAS No.:1237587-26-6
Molecular Formula:C₂₀H₁₅Cl₃F₃N₃O₂
Molecular Weight:492.712
Hs Code.:

Synonyms:N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

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Chemical Property of N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

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Technology Process of N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

There total 17 articles about N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1415107-37-7
2-{2-chloro-5-[3-(3,5-dichlorophenyl)-4,4,4-trifluoro-1-oxo-2-buten-1-yl]phenyl}cyclopropanecarbohydrazide

: 1237587-26-6
N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Guidance literature:: With hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium hydroxide; In tert-butyl methyl ether; water; at 20 ℃; for 72h;

Reference yield:

: 1237587-25-5
tert-butyl N'-cyclopropanecarbonyl-N-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

: 1237587-26-6
N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Guidance literature:: tert-butyl N'-cyclopropanecarbonyl-N-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate; With trifluoroacetic acid; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield:

: 66399-01-7
2-chloro-5-hydroxyiminomethylnitrobenzene

: 1237587-26-6
N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}cyclopropanecarbohydrazide

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: acetic acid; iron / ethanol; water / 0.83 h / 75 °C

3.1: toluene; tetrahydrofuran / 1 h / 80 °C

3.2: 16 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 20 °C

4.2: 15 h / 20 °C

5.1: triethylamine / water; tetrahydrofuran / 1 h / 20 °C

6.1: trifluoroacetic acid / 1 h / 20 °C

With N-chloro-succinimide; iron; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene; mineral oil;