1,3-diphenyl-4-propylisoquinoline

Base Information

Chemical Name:1,3-diphenyl-4-propylisoquinoline
CAS No.:1295521-98-0
Molecular Formula:C₂₄H₂₁N
Molecular Weight:323.437
Hs Code.:

Synonyms:1,3-diphenyl-4-propylisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-diphenyl-4-propylisoquinoline

Chemical Property:

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Technology Process of 1,3-diphenyl-4-propylisoquinoline

There total 5 articles about 1,3-diphenyl-4-propylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 4250-81-1
1-phenyl-1-pentyne

: 574-66-3
Benzophenone oxime

: 1295521-98-0
1,3-diphenyl-4-propylisoquinoline

: 75097-27-7
3-n-propyl-1,4-diphenylisoquinoline

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; In methanol; at 60 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000887

Reference yield: 26.0%

: 891782-22-2
N-tert-butylsulfinyl ketoimine

: 4250-81-1
1-phenyl-1-pentyne

: 1295521-98-0
1,3-diphenyl-4-propylisoquinoline

: 75097-27-7
3-n-propyl-1,4-diphenylisoquinoline

Guidance literature:: N-tert-butylsulfinyl ketoimine; 1-phenyl-1-pentyne; With CoCp*(CO)I₂; acetic acid; silver(I) triflimide; In 1,2-dichloro-ethane; at 120 ℃; for 18h; Inert atmosphere; Sealed tube;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h; Overall yield = 69 %;
DOI:10.1016/S1872-2067(16)62491-9

Reference yield:

: 119-61-9
benzophenone

: 1295521-98-0
1,3-diphenyl-4-propylisoquinoline

: 75097-27-7
3-n-propyl-1,4-diphenylisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; hydroxylamine hydrochloride / 8 h / 20 °C

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate / methanol / 16 h / 60 °C / Inert atmosphere

With pyridine; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; hydroxylamine hydrochloride; cesium acetate; In methanol;
DOI:10.1002/adsc.201000887