tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate

Base Information

Chemical Name:tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate
CAS No.:1287206-23-8
Molecular Formula:C₁₇H₂₇BrN₂O₂
Molecular Weight:371.318
Hs Code.:

Synonyms:tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate

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Chemical Property of tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate

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Technology Process of tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate

There total 1 articles about tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118171-79-2,141321-51-9,141321-54-2,87694-55-1
N-(t-butoxycarbonyl)-isoleucine aldehyde

: 106-40-1
4-bromo-aniline

: 1287206-23-8
tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;
DOI:10.1021/cn500082p DOI:10.1021/acschemneuro.6b00182

Reference yield: 80.0%

: trans-2-(6-fluoropyridin-2yl)cyclopropanecarboxylic acid

: 1287206-23-8
tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate

: 1287206-05-6
[(1S,2S)-1-({(4-bromophenyl)[trans-2-(6-fluoropyridin-2-yl)cyclopropanecarbonyl]amino}methyl)-2-methylbutyl]carbamic acid tert-butyl ester

Guidance literature:: trans-2-(6-fluoropyridin-2yl)cyclopropanecarboxylic acid; With thionyl chloride; Reflux;

tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate; With triethylamine; In dichloromethane; at 20 ℃;

Reference yield: 75.0%

: 3471-10-1
(1R,2R)-trans-2-phenyl-1-cyclopropanecarboxylic acid

: 1287206-23-8
tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate

: tert-butyl [(2S,3S)-1-{4-bromophenyl[(1R,2R)-2-phenyl-1-cyclopropanecarbonyl]amino}-3-methylpentan-2-yl]carbamate

Guidance literature:: (1R,2R)-trans-2-phenyl-1-cyclopropanecarboxylic acid; With thionyl chloride; Reflux;

tert-butyl {(2S,3S)-1-[(4-bromophenyl)amino]-3-methylpentan-2-yl}carbamate; With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/cn500082p