amino-bis-trifluoromethyl-phosphine

Base Information

• Chemical Name: amino-bis-trifluoromethyl-phosphine
• CAS No.: 431-95-8
• Molecular Formula: C₂H₂F₆NP
• Molecular Weight: 185.009

Synonyms:amino-bis-trifluoromethyl-phosphine

Chemical Property of amino-bis-trifluoromethyl-phosphine

Chemical Property:

Purity/Quality:

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Technology Process of amino-bis-trifluoromethyl-phosphine

There total 4 articles about amino-bis-trifluoromethyl-phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tris(trifluoromethyl)phosphine (432-04-2) → trifluoromethan (75-46-7) + amino-bis-trifluoromethyl-phosphine (431-95-8)

Guidance literature:

ammonolysis at 22°C (157 Torr), finally condensation to -70°C (30 min) and warming to 20°C;

DOI:10.1039/JR9580000512

Reference yield:

tris(trifluoromethyl)phosphine (432-04-2) + ammonia (7664-41-7) → trifluoromethan (75-46-7) + amino-bis-trifluoromethyl-phosphine (431-95-8)

Guidance literature:

DOI:10.1039/jr9580000512

Reference yield:

Tris--amin (2071-50-3) → amino-bis-trifluoromethyl-phosphine (431-95-8) + Bis{bis(trifluormethyl)phosphanyl}amin (2349-17-9)

Guidance literature:

With NH₃; 24°C; unsuccessful quantitative sepn.;

upstream raw materials:

tris(trifluoromethyl)phosphine

ammonia

bis(trifluoromethyl)phosphine

Tris--amin

Downstream raw materials:

Bis{bis(trifluormethyl)phosphanyl}amin

chlorotrifluoromethane

bis(trifluoromethyl)trichlorophosphorane

trifluoromethan

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