[3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester

Base Information

• Chemical Name: [3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester
• CAS No.: 87544-32-9
• Molecular Formula: C₂₂H₂₆N₂O₃S
• Molecular Weight: 398.526

Synonyms:[3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester

Chemical Property of [3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

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Technology Process of [3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester

There total 1 articles about [3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium thioacyanate (333-20-0) + benzoyl chloride (98-88-4) + (2,6-Dimethyl-phenylamino)-acetic acid tert-butyl ester → [3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester (87544-32-9)

Guidance literature:

Yield given. Multistep reaction; 1.) acetone, reflux, 5 min 2.) acetone, rt.; refux, 2 h;

Reference yield: 76.0%

[3-Benzoyl-1-(2,6-dimethyl-phenyl)-thioureido]-acetic acid tert-butyl ester (87544-32-9) → 1-(2,6-dimethylphenyl)thiourea (6396-76-5) + 3-(2,6-Dimethyl-phenyl)-5-phenyl-2-thioxo-2,3-dihydro-1H-imidazole-4-carboxylic acid tert-butyl ester (87544-49-8)

Guidance literature:

With potassium hydroxide; In ethanol; water; for 2h; Heating;

upstream raw materials:

potassium thioacyanate

benzoyl chloride

Downstream raw materials:

1-(2,6-dimethylphenyl)thiourea

3-(2,6-Dimethyl-phenyl)-5-phenyl-2-thioxo-2,3-dihydro-1H-imidazole-4-carboxylic acid tert-butyl ester

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