1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Base Information

Chemical Name:1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
CAS No.:1338233-12-7
Molecular Formula:C₁₆H₁₁N₃O₆
Molecular Weight:341.28
Hs Code.:

Synonyms:1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

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Chemical Property of 1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Chemical Property:

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Technology Process of 1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

There total 5 articles about 1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1195-08-0
2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

: 40941-60-4
2-(bromomethyl)-5-(2-nitrophenyl)furan

: 1338233-12-7
1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 8h;
DOI:10.1016/j.bmcl.2011.07.107

Reference yield:

: 40105-90-6
[5-(2-nitrophenyl)furan-2-yl]methanol

: 1338233-12-7
1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide / dichloromethane / 0 - 25 °C

2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 50 °C

With phosphorus tribromide; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.107

Reference yield:

: 5570-19-4
2-nitrophenylboronic acid

: 1338233-12-7
1-((5-(2-nitrophenyl)furan-2-yl)methyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 3 h / 120 °C

2: sodium tetrahydroborate / ethanol / 0 - 25 °C

3: phosphorus tribromide / dichloromethane / 0 - 25 °C

4: potassium carbonate / N,N-dimethyl-formamide / 8 h / 50 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; potassium carbonate; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2011.07.107