N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester
CAS No.:1433903-58-2
Molecular Formula:C₃₁H₂₁Cl₂N₃O₃
Molecular Weight:554.432
Hs Code.:

Synonyms:N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

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Chemical Property of N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

There total 5 articles about N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 35661-51-9
N-(9-fluorenylmethyloxycarbonyl)hydrazine

: 2,6-dichloro-4-phenylquinoline-3-carbonyl chloride

: 1433903-58-2
N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/j.bmcl.2016.08.071

Reference yield:

: 35661-51-9
N-(9-fluorenylmethyloxycarbonyl)hydrazine

: 94205-21-7
6-chloro-2-oxo-4-phenyl-1,2-dihydro-quinoline-3-carboxylic acid

: 1433903-58-2
N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: 6-chloro-2-oxo-4-phenyl-1,2-dihydro-quinoline-3-carboxylic acid; With trichlorophosphate; at 120 ℃; for 3h;

N-(9-fluorenylmethyloxycarbonyl)hydrazine; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 284663-87-2
6-chloro-2-oxo-4-phenyl-1,2-dihydro-quinoline-3-carboxylic acid methyl ester

: 1433903-58-2
N'-(2,6-dichloro-4-phenyl-quinoline-3-carbonyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide / ethanol / 72 h / 50 °C / Sealed tube

2.1: trichlorophosphate / 3 h / 120 °C

2.2: 4 h / 20 °C

With lithium hydroxide; trichlorophosphate; In ethanol;