COPPER(II) 5,9,14,18,23,27,32,36-OCTABUTOXY-2,3-NAPHTHALOCYANINE

Base Information

• Chemical Name: COPPER(II) 5,9,14,18,23,27,32,36-OCTABUTOXY-2,3-NAPHTHALOCYANINE
• CAS No.: 155773-67-4
• Molecular Formula: C₈₀H₈₈CuN₈O₈
• Molecular Weight: 1353.17
• Mol file: 155773-67-4.mol

Synonyms:Copper,[5,9,14,18,23,27,32,36-octabutoxy-37H,39H-tetranaphtho[2,3-b:2',3'-g:2'',3''-l:2''',3'''-q]porphyrazinato(2-)-N37,N38,N39,N40]-,(SP-4-1)-;37H,39H-Tetranaphtho[2,3-b:2',3'-g:2'',3''-l:2''',3'''-q]porphyrazine, copperderiv.

Chemical Property of COPPER(II) 5,9,14,18,23,27,32,36-OCTABUTOXY-2,3-NAPHTHALOCYANINE

Chemical Property:

• PSA: 157.86000
• LogP: 15.50590

Purity/Quality:

98%,99%, ^*data from raw suppliers

Copper(II) 5,9,14,18,23,27,32,36-Octabutoxy-2,3-naphthalocyanine >97.0%(N)(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of COPPER(II) 5,9,14,18,23,27,32,36-OCTABUTOXY-2,3-NAPHTHALOCYANINE

There total 2 articles about COPPER(II) 5,9,14,18,23,27,32,36-OCTABUTOXY-2,3-NAPHTHALOCYANINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

copper diacetate (142-71-2) + 5,9,14,18,23,27,32,36-octa-n-butoxy-2,3-naphthalocyanine (105528-25-4) → C80H88CuN8O8 (155773-67-4)

Guidance literature:

In tetrahydrofuran; at 60 ℃; for 4h;

Reference yield: 62.0%

5,9,14,18,23,27,32,36-octabutoxy-2,3-napthalocyanine (105528-25-4) + copper(II) acetate monohydrate (6046-93-1) → Cu(5,9,14,18,23,27,32,36-octabutoxynaphthalocyanine(2-)) (155773-67-4)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In butan-1-ol; under Ar atm. mixt. Co(OAc)2*4H2O, naphthalocyanine, 1,8-diazabicyclo(5.4.0)undec-7-ene and 1-butanol was refluxed for 20 h; react. mixt. was diluted with MeOH and H2O, ppt. was filtered and chromed. on Al2O3-V (toluene), vac.-dried at room temp.;

DOI:10.1021/ic7023204

upstream raw materials:

5,9,14,18,23,27,32,36-octabutoxy-2,3-napthalocyanine

copper(II) acetate monohydrate

copper diacetate

5,9,14,18,23,27,32,36-octa-n-butoxy-2,3-naphthalocyanine

Refernces

• 1、 -. "METHOD OF PROVING AUTHENTICITY, SIGNAL CONVERSION METHOD, POLYMER WELDING METHOD, METHOD OF PRODUCING LITHOGRAPHIC PRINTING PLATE, INK FOR PRINTING, TONER, AND HEAT RAY-SHIELDING MATERIAL, EACH USING NAPHTHALOCYANINE COMPOUND, AND METHOD OF PRODUCING NAPHTHALOCYANINE COMPOUND". Page/Page column 29. . Retrieved 2012/01/12.