2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide

Base Information

Chemical Name:2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide
CAS No.:515875-68-0
Molecular Formula:C₁₆H₁₈N₄O₃S
Molecular Weight:346.41
Hs Code.:

Synonyms:2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide

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Chemical Property of 2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide

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Technology Process of 2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide

There total 4 articles about 2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 126087-33-0
ethyl (5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl)thioacetate

: 515875-68-0
2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Heating;
DOI:10.1080/10426500214894 DOI:10.1002/jccs.200200152

Reference yield:

: 626-34-6
ethyl 3-aminobut-2-enoate

: 515875-68-0
2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / acetone / 2 h / Heating

2: AcONa / ethanol / 2 h / Heating

3: 82 percent / hydrazine hydrate / ethanol / 1 h / Heating

With sodium acetate; hydrazine hydrate; In ethanol; acetone;
DOI:10.1002/jccs.200200152

Reference yield:

: 532-55-8
Benzoyl isothiocyanate

: 515875-68-0
2-[5-ethoxycarbonyl-4-methyl-2-phenylpyrimidin-6-yl]mercaptoacetichydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / acetone / 2 h / Heating

2: AcONa / ethanol / 2 h / Heating

3: 82 percent / hydrazine hydrate / ethanol / 1 h / Heating

With sodium acetate; hydrazine hydrate; In ethanol; acetone;
DOI:10.1002/jccs.200200152