α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene

Base Information

• Chemical Name: α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene
• CAS No.: 108149-81-1
• Molecular Formula: C₃₀H₃₄O₉S₂
• Molecular Weight: 602.727
• Mol file: 108149-81-1.mol

Synonyms:α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene

Chemical Property of α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene

There total 1 articles about α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

methanesulfonyl chloride (124-63-0) + α,α-bis(2-hydroxy-6-isopropyltropon-3-yl)-4-methoxytoluene (92832-17-2) → α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene (108149-81-1)

Guidance literature:

With triethylamine; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1021/jm00390a022

Reference yield: 81.0%

α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene (108149-81-1) → α,α-bis(2-hydroxy-5-isopropyl-3-thioxo-1,4,6-cycloheptatrienyl)-4-methoxytoluene (108149-82-2)

Guidance literature:

With sodium hydrogensulfide; In N,N-dimethyl-formamide; for 9h; Ambient temperature;

DOI:10.1021/jm00390a022

Reference yield: 71.0%

α,α-bis<4-isopropyl-2-(mesyloxy)tropon-7-yl>-4-methoxytoluene (108149-81-1) + methylamine (74-89-5) → α-<4-isopropyl-2-(N-methylamino)tropon-7-yl>-α-(2-hydroxy-6-isopropyltropon-3-yl)-4-methoxytoluene (108149-85-5)

Guidance literature:

In methanol; acetonitrile; for 4h; Ambient temperature;

DOI:10.1021/jm00390a022

upstream raw materials:

methanesulfonyl chloride

α,α-bis(2-hydroxy-6-isopropyltropon-3-yl)-4-methoxytoluene

Downstream raw materials:

α,α-bis(2-hydroxy-5-isopropyl-3-thioxo-1,4,6-cycloheptatrienyl)-4-methoxytoluene

α-<4-isopropyl-2-(N-methylamino)tropon-7-yl>-α-(2-hydroxy-6-isopropyltropon-3-yl)-4-methoxytoluene

α,α-bis<4-isopropyl-2-(N-methylamino)tropon-7-yl>-4-methoxytoluene