C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO

Base Information

Chemical Name:C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO
CAS No.:251302-09-7
Molecular Formula:C₂₂H₂₅NO₃
Molecular Weight:351.445
Hs Code.:

C<sub>5</sub>H<sub>7</sub>CO<sub>2</sub>CH<sub>3</sub>NC<sub>6</sub>H<sub>5</sub>C<sub>2</sub>H<sub>4</sub>C<sub>6</sub>H<sub>5</sub>CHO

Synonyms:C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO

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Chemical Property of C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO

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Technology Process of C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO

There total 3 articles about C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 100-52-7
benzaldehyde

: 251302-01-9
(1S,3R,4R)-2-benzyl-2-azabicyclo[2.2.1]heptane-3-carboxylic acid methyl ester

: 251302-09-7
C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO

Guidance literature:: (1S,3R,4R)-2-benzyl-2-azabicyclo[2.2.1]heptane-3-carboxylic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -20 ℃; for 0.666667h;

benzaldehyde; In tetrahydrofuran; at -5 - 20 ℃; Further stages.;
DOI:10.1021/ol990942c

Reference yield:

: 130195-74-3
(1R,3R,4S)-2-[(1S)-1-phenylethyl]-2-azabicyclo[2.2.1]hept-5-ene-3-carboxylic acid methyl ester

: 251302-09-7
C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂ / Pd/C / methanol / 20 °C / 5320.36 Torr

2.1: K₂CO₃ / acetonitrile / 20 °C

3.1: LDA / tetrahydrofuran / 0.67 h / -20 °C

3.2: 68 percent / tetrahydrofuran / -5 - 20 °C

With hydrogen; potassium carbonate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ol990942c

Reference yield:

: 297143-31-8,220093-41-4
(1S,3R,4R)-2-azabicyclo[2.2.1]heptane-3-carboxylic acid methyl ester

: 251302-09-7
C₅H₇CO₂CH₃NC₆H₅C₂H₄C₆H₅CHO

Guidance literature:: Multi-step reaction with 2 steps

1.1: K₂CO₃ / acetonitrile / 20 °C

2.1: LDA / tetrahydrofuran / 0.67 h / -20 °C

2.2: 68 percent / tetrahydrofuran / -5 - 20 °C

With potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol990942c