Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

Base Information

Chemical Name:Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂
CAS No.:86857-67-2
Molecular Formula:C₂₆H₂₆Cl₂MoS₂
Molecular Weight:569.47
Hs Code.:

Mo(C<sub>5</sub>H<sub>4</sub>CH<sub>2</sub>CH<sub>2</sub>SC<sub>6</sub>H<sub>5</sub>)2Cl<sub>2</sub>

Synonyms:Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

Suppliers and Price of Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

There total 1 articles about Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: Mo(C₅H₄CH₂CH₂SC₆H₅)2(SC₆H₅)2

: 86857-67-2
Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

Guidance literature:: With hydrogenchloride; In dichloromethane; Mo complex treated with HCl gas in CH2Cl2 for 1 h; evapn., crystn. (CH2Cl2-light petroleum); elem. anal.;
DOI:10.1039/DT9830000861

Reference yield: 51.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 86857-67-2
Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

: 98183-65-4
[μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate

Guidance literature:: In acetone; (inert gas); to suspn. of Mo complex was added soln. of Rh complex and stirred for 4 h at 40°C; cool soln. was evapd. in vac., residue extd. with acetone, concd. soln.was cooled to -78°C, yielding green powder within 24 h, it was washed with Et2O and dried in vac.; elem. anal.;
DOI:10.1016/0022-328X(85)87172-2

Reference yield: 37.0%

: ammonium hexafluorophosphate

: 86857-67-2
Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

: 86857-58-1
chloro[η5-(2-phenylthioethyl)cyclopentadienyl][η5-(2-phenylthioethyl)cyclopentadienyl-S]molybdenum hexafluorophosphate

Guidance literature:: With FeCl₂*1.5THF; In tetrahydrofuran; water; FeCl2*1.5THF under inert gas added to Mo complex in THF, heated to 50°C for 1 h, evapd., extd. with H2O, filtered, excess aq. NH4PF6 added; washing with H2O, drying in vac., recrystn. (acetone-H2O); elem. anal.;
DOI:10.1039/DT9830000861