(1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester

Base Information

• Chemical Name: (1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester
• CAS No.: 145414-37-5
• Molecular Formula: C₂₀H₂₀O₃
• Molecular Weight: 308.377

Synonyms:(1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester

Chemical Property of (1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester

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Technology Process of (1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester

There total 4 articles about (1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

5-(2,2-diphenylvinyl)-2-oxabicyclo<2.1.1>hexan-3-one (92776-59-5) → methyl cis-3-hydroxy-2-(2,2-diphenylvinyl)cyclobutane-1-carboxylate (92776-60-8,145414-37-5,145414-38-6)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; for 22h; Ambient temperature;

Reference yield: 85.0%

methanol (67-56-1) → (1R,2S,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester (145414-38-6) + (1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester (145414-37-5)

Guidance literature:

toluene-4-sulfonic acid; for 12h; Ambient temperature;

Reference yield: 8.0%

methanol (67-56-1) + (1S,4R,5S)-5-(2,2-Diphenyl-vinyl)-2-oxa-bicyclo[2.1.1]hexan-3-one (92776-59-5,145414-36-4) → (1R,2S,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester (145414-38-6) + (1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarboxylic acid methyl ester (145414-37-5)

Guidance literature:

toluene-4-sulfonic acid; for 12h; Ambient temperature;

upstream raw materials:

methanol

5-(2,2-diphenylvinyl)-2-oxabicyclo<2.1.1>hexan-3-one

(1S,4R,5S)-5-(2,2-Diphenyl-vinyl)-2-oxa-bicyclo[2.1.1]hexan-3-one

Downstream raw materials:

(1S,2R,3R)-2-(2,2-Diphenyl-vinyl)-3-hydroxymethyl-cyclobutanol

(1R,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarbaldehyde

(1S,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxy-cyclobutanecarbaldehyde

(1S,2R,3S)-2-(2,2-Diphenyl-vinyl)-3-hydroxymethyl-cyclobutanol

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