BrC₆H₄COOCH₂C₁₄H₈CH₂OCOC₆H₄Br

Base Information

• Chemical Name: BrC₆H₄COOCH₂C₁₄H₈CH₂OCOC₆H₄Br
• CAS No.: 309928-75-4
• Molecular Formula: C₃₀H₂₀Br₂O₄
• Molecular Weight: 604.294
• Mol file: 309928-75-4.mol

Synonyms:BrC₆H₄COOCH₂C₁₄H₈CH₂OCOC₆H₄Br

Chemical Property of BrC₆H₄COOCH₂C₁₄H₈CH₂OCOC₆H₄Br

Chemical Property:

Purity/Quality:

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Technology Process of BrC₆H₄COOCH₂C₁₄H₈CH₂OCOC₆H₄Br

There total 1 articles about BrC₆H₄COOCH₂C₁₄H₈CH₂OCOC₆H₄Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3-bromobenzoyl chloride (1711-09-7) + 9,1-bis(chloromethyl)anthracene (10387-13-0) → BrC6H4COOCH2C14H8CH2OCOC6H4Br (309928-75-4)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 35 ℃; for 20h;

DOI:10.1021/ol0065625

Reference yield:

methanol (67-56-1) + tributylphenylstannane (960-16-7) + BrC6H4COOCH2C14H8CH2OCOC6H4Br (309928-75-4) → methyl 3-phenylbenzoate (16606-00-1)

Guidance literature:

tributylphenylstannane; BrC₆H₄COOCH₂C₁₄H₈CH₂OCOC₆H₄Br; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 100 ℃; for 12h;

With N-benzylmaleimide resin; at 90 ℃; for 3h;

methanol; With sodium methylate; In tetrahydrofuran; Further stages.;

DOI:10.1021/ol0065625

upstream raw materials:

3-bromobenzoyl chloride

9,1-bis(chloromethyl)anthracene

Downstream raw materials:

methyl 3-phenylbenzoate