1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Base Information

Chemical Name:1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)
CAS No.:1352127-37-7
Molecular Formula:C₃₆H₄₆N₄O₁₄
Molecular Weight:758.78
Hs Code.:

1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Synonyms:1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Suppliers and Price of 1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

There total 6 articles about 1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1352127-36-6
4-(4-(1-(methacryloyloxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

: 107-15-3,85404-18-8
ethylenediamine

: 1352127-37-7
1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 25 ℃; for 15h;
DOI:10.1021/ma201706r

Reference yield:

: 498-02-2
1-(3-methoxy-4-hydroxyphenyl)ethanone

: 1352127-37-7
1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 25 °C

2: nitric acid; acetic anhydride / 3 h / 0 °C

3: sodium tetrahydroborate / tetrahydrofuran; methanol / 16 h / 25 °C

4: sodium hydroxide / tetrahydrofuran; methanol / 7 h / 25 °C

5: triethylamine / dichloromethane / 15 h / 0 - 25 °C / Inert atmosphere

6: dmap; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 0 - 25 °C

With dmap; sodium tetrahydroborate; nitric acid; acetic anhydride; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ma201706r

Reference yield:

: 175281-79-5
methyl 4-(4-acetyl-2-methoxyphenoxy)butanoate

: 1352127-37-7
1,1'-(4,4'-(4,4'-(ethane-1,2-diylbis(azanediyl))bis(4-oxobutane-4,1-diyl))bis(oxy)bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methyl acrylate)

Guidance literature:: Multi-step reaction with 5 steps

1: nitric acid; acetic anhydride / 3 h / 0 °C

2: sodium tetrahydroborate / tetrahydrofuran; methanol / 16 h / 25 °C

3: sodium hydroxide / tetrahydrofuran; methanol / 7 h / 25 °C

4: triethylamine / dichloromethane / 15 h / 0 - 25 °C / Inert atmosphere

5: dmap; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 0 - 25 °C

With dmap; sodium tetrahydroborate; nitric acid; acetic anhydride; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ma201706r