phenylacetylene-2-13C-2-2H

Base Information

Chemical Name:phenylacetylene-2-13C-2-2H
CAS No.:91230-89-6
Molecular Formula:C₈H₆
Molecular Weight:104.117
Hs Code.:

Synonyms:phenylacetylene-2-13C-2-2H

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Chemical Property of phenylacetylene-2-13C-2-2H

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Technology Process of phenylacetylene-2-13C-2-2H

There total 5 articles about phenylacetylene-2-13C-2-2H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 54522-92-8
phenylacetylene-2-13C

: 91230-89-6
phenylacetylene-2-13C-2-2H

Guidance literature:: With deuteriated sodium hydroxide; water-d2; cetyldimethylbenzylammonium chloride; In dichloromethane;
DOI:10.1021/ja00330a046

Reference yield:

: 71777-36-1
acetophenone-β-¹³C

: 91230-89-6
phenylacetylene-2-13C-2-2H

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅ / benzene / 5 h / 0 °C

2: NaNH₂ / liquid ammonia; diethyl ether / 3 h / -78 °C

3: 87 percent / D₂O, benzylhexadecyldimethylammonium chloride, NaOD / CH₂Cl₂

With deuteriated sodium hydroxide; phosphorus pentachloride; water-d2; cetyldimethylbenzylammonium chloride; sodium amide; In diethyl ether; dichloromethane; ammonia; benzene;
DOI:10.1021/ja00330a046

Reference yield:

: 100-52-7
benzaldehyde

: 91230-89-6
phenylacetylene-2-13C-2-2H

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) tert-butyllithium / 1.) pentane, -78 deg C, 2.45 h; 2.) pentane, ether, -78 deg C, 7 h

2: PCC / CH₂Cl₂

3: PCl₅ / benzene / 5 h / 0 °C

4: NaNH₂ / liquid ammonia; diethyl ether / 3 h / -78 °C

5: 87 percent / D₂O, benzylhexadecyldimethylammonium chloride, NaOD / CH₂Cl₂

With deuteriated sodium hydroxide; phosphorus pentachloride; water-d2; tert.-butyl lithium; cetyldimethylbenzylammonium chloride; sodium amide; pyridinium chlorochromate; In diethyl ether; dichloromethane; ammonia; benzene;
DOI:10.1021/ja00330a046