3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline

Base Information

Chemical Name:3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline
CAS No.:955009-86-6
Molecular Formula:C₄₃H₄₆N₄O₂
Molecular Weight:650.864
Hs Code.:

Synonyms:3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline

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Chemical Property of 3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline

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Technology Process of 3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline

There total 12 articles about 3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: N,N-dibenzyl-N'-methylpentane-1,5-diamine

: 839672-50-3
methyl 3-[2-((4-biphenyl)iminomethyleneamino)phenyl]acrylate

: 955009-86-6
3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline

Guidance literature:: In toluene; for 2h;

Reference yield: 99.0%

: N,N-dibenzyl-N'-methylpentane-1,5-diamine

: methyl trans-2-(3-biphenylcarbodiimido)cinnamate

: 955009-86-6
3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline

Guidance literature:: In toluene; at 20 ℃;
DOI:10.1016/j.bmcl.2007.08.070

Reference yield:

: 51644-96-3
5-tert-butoxycarbonylamino-1-aminopentane

: 955009-86-6
3-biphenyl-4-yl-2-[(5-N,N-dibenzylaminopentyl)-N'-methylamino]-4-methoxycarbonylmethyl-3,4-dihydroquinazoline

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / dichloromethane / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

2.2: 0 °C

3.1: toluene / 1 h / 20 °C

With lithium aluminium tetrahydride; sodium carbonate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.5012/bkcs.2010.31.11.3353