methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate

Base Information

Chemical Name:methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate
CAS No.:457612-43-0
Molecular Formula:C₂₁H₂₅O₅P
Molecular Weight:388.4
Hs Code.:

Synonyms:methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate

Chemical Property:

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Technology Process of methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate

There total 1 articles about methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67-56-1
methanol

: 457612-42-9
(1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylic acid

: 457612-43-0
methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate

Guidance literature:: With sulfuric acid; for 12h; Heating;
DOI:10.1021/jo025725v

Reference yield: 93.0%

: 457612-43-0
methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate

: methyl (1R,2S,3S,5S)-5-(diphenylphosphino)-2,3-dimethoxycyclopentanecarboxylate

Guidance literature:: With trichlorosilane; triethylamine; In benzene; at 0 - 110 ℃; for 24h;
DOI:10.1021/jo025725v

Reference yield:

: 457612-43-0
methyl (1R,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentanecarboxylate

: (1R,2S,3S,5S)-5-(diphenylphosphino)-2,3-dimethoxycyclopentanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / trichlorosilane; triethylamine / benzene / 24 h / 0 - 110 °C

2: 98 percent / sodium hydroxide / tetrahydrofuran; H₂O / 12 h / 50 °C

With sodium hydroxide; trichlorosilane; triethylamine; In tetrahydrofuran; water; benzene;
DOI:10.1021/jo025725v