dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine

Base Information

Chemical Name:dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine
CAS No.:882426-55-3
Molecular Formula:C₃₆H₃₅Br₃N₄O₃
Molecular Weight:811.411
Hs Code.:

Synonyms:dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine

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Chemical Property of dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine

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Technology Process of dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine

There total 5 articles about dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 83004-10-8
2-bromo-6-bromomethylpyridine

: 175724-27-3
N,N-dibenzyl tris(hydroxymethyl)aminomethane

: 882426-55-3
dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 25 ℃; for 1h;
DOI:10.1016/j.tetlet.2006.01.026

Reference yield: 41.0%

: 83004-10-8
2-bromo-6-bromomethylpyridine

: 175724-27-3
N,N-dibenzyl tris(hydroxymethyl)aminomethane

: 3-(6-bromo-pyridin-2-ylmethoxy)-2-(6-bromo-pyridin-2-ylmethoxymethyl)-2-dibenzylamino-propan-1-ol

: 882426-55-3
dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 65 ℃; for 28h;
DOI:10.1016/j.tetlet.2006.01.026

Reference yield:

: 1824-81-3
2-Amino-6-methylpyridine

: 882426-55-3
dibenzyl-[2-(6-bromo-pyridin-2-ylmethoxy)-1,1-bis-(6-bromo-pyridin-2-ylmethoxymethyl)-ethyl]-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: HBr; Br₂ / -20 °C

1.2: 79 percent / NaNO₂ / 0 °C

2.1: 67 percent / NBS; AIBN / CH₂Cl₂; H₂O / Heating

3.1: 41 percent / NaH / tetrahydrofuran / 28 h / 65 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydrogen bromide; bromine; sodium hydride; In tetrahydrofuran; dichloromethane; water; 1.1: Sandmeyer reaction;
DOI:10.1016/j.tetlet.2006.01.026