Technology Process of C18H25NO5
There total 4 articles about C18H25NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
acetone; toluene;
at 20 ℃;
Concentration;
Large scale;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium tert-butylate / tetrahydrofuran / 0 - 10 °C
2: dipotassium hydrogenphosphate; alpha-D-glucopyranose; NADP; GDH-105; CDX-018; sodium hydroxide / water; dimethyl sulfoxide / 48 h / 30 - 35 °C / pH 7.3 - 7.7 / Enzymatic reaction
3: boron trifluoride diethyl etherate / toluene; acetone / 17 h / 20 °C
With
dipotassium hydrogenphosphate; alpha-D-glucopyranose; CDX-018; GDH-105; boron trifluoride diethyl etherate; potassium tert-butylate; NADP; sodium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide; acetone; toluene;
1: |Chan Rearrangement;
DOI:10.1021/ol400252p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dipotassium hydrogenphosphate; alpha-D-glucopyranose; NADP; GDH-105; CDX-018; sodium hydroxide / water; dimethyl sulfoxide / 48 h / 30 - 35 °C / pH 7.3 - 7.7 / Enzymatic reaction
2: boron trifluoride diethyl etherate / toluene; acetone / 17 h / 20 °C
With
dipotassium hydrogenphosphate; alpha-D-glucopyranose; CDX-018; GDH-105; boron trifluoride diethyl etherate; NADP; sodium hydroxide;
In
water; dimethyl sulfoxide; acetone; toluene;
DOI:10.1021/ol400252p
