4-Chloro-5-fluoro-2-nitrobenzoic Acid Methyl Ester

Base Information

• Chemical Name: 4-Chloro-5-fluoro-2-nitrobenzoic Acid Methyl Ester
• CAS No.: 1113049-81-2
• Molecular Formula: C₈H₅ClFNO₄
• Molecular Weight: 233.583
• Mol file: 1113049-81-2.mol

Synonyms:C₈H₅ClFNO₄

Chemical Property of 4-Chloro-5-fluoro-2-nitrobenzoic Acid Methyl Ester

Chemical Property:

• Boiling Point: 301.4±42.0 °C(Predicted)
• Density: 1.503±0.06 g/cm3(Predicted)
• Storage Temp.: 2-8°C
• Solubility.: DCM, Ethyl Acetate,

Purity/Quality:

97% ^*data from raw suppliers

4-Chloro-5-fluoro-2-nitrobenzoicAcidMethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 4-Chloro-5-fluoro-2-nitrobenzoic Acid Methyl Ester is an intermediate in the synthesis of Albaconazole (H761395), an antifungal agent as neuroprotectant.

Technology Process of 4-Chloro-5-fluoro-2-nitrobenzoic Acid Methyl Ester

There total 1 articles about 4-Chloro-5-fluoro-2-nitrobenzoic Acid Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 4-chloro-3-fluorobenzoic acid (403-17-8) → C8H5ClFNO4 (1113049-81-2)

Guidance literature:

4-chloro-3-fluorobenzoic acid; With sulfuric acid; sodium nitrite; at 0 - 20 ℃;

methanol; at 0 - 100 ℃; for 4.5h;

Reference yield:

C8H5ClFNO4 (1113049-81-2) → C8H6ClNO5 (1113049-82-3)

Guidance literature:

C₈H₅ClFNO₄; With 2-(methylsulfonyl)ethyl alcohol; sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;

With hydrogenchloride; water; In N,N-dimethyl-formamide;

upstream raw materials:

methanol

4-chloro-3-fluorobenzoic acid

Downstream raw materials:

C₈H₆ClNO₅

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