Technology Process of C30H40O3Si
There total 14 articles about C30H40O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
aq. phosphate buffer;
DOI:10.1021/ol201547q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere
1.2: 0 °C / Inert atmosphere
1.3: 0 °C / Inert atmosphere; Saturated solution
2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / 20 °C / Inert atmosphere; Molecular sieve
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 - 20 °C / aq. phosphate buffer
With
n-butyllithium; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol201547q
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium periodate / tetrahydrofuran; water / 0.17 h / 20 °C / Inert atmosphere
2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere
4.2: 0 °C / Inert atmosphere
4.3: 0 °C / Inert atmosphere; Saturated solution
5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / 20 °C / Inert atmosphere; Molecular sieve
6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 - 20 °C / aq. phosphate buffer
With
sodium periodate; n-butyllithium; tetrapropylammonium perruthennate; carbon tetrabromide; 4-methylmorpholine N-oxide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1021/ol201547q