3-morpholino-1-phenylpropan-1-one

Base Information

• Chemical Name: 3-morpholino-1-phenylpropan-1-one
• CAS No.: 2298-48-8
• Molecular Formula: C13H17NO2
• Molecular Weight: 219.283
• Hs Code.: 2934999090
• Mol file: 2298-48-8.mol

Synonyms:Propiophenone,3-morpholino- (6CI,7CI,8CI);3-(4-Morpholinyl)-1-phenyl-1-propanone;3-Morpholino-1-phenylpropan-1-one;b-Morpholinopropiophenone;

Chemical Property of 3-morpholino-1-phenylpropan-1-one

Chemical Property:

• Vapor Pressure: 2.83E-05mmHg at 25°C
• Melting Point: 178-180℃
• Boiling Point: 356.9 °C at 760 mmHg
• Flash Point: 169.7 °C
• PSA: 29.54000
• Density: 1.085 g/cm³
• LogP: 1.52950
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3-Morpholino-1-phenylpropan-1-one 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-morpholino-1-phenylpropan-1-one

There total 21 articles about 3-morpholino-1-phenylpropan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

morpholine (110-91-8,99108-56-2) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + acetophenone (98-86-2) → 3-morpholin-4-yl-1-phenyl-propan-1-one (2298-48-8)

Guidance literature:

With C₇H₁₃N₂O₃S⁽¹⁺⁾*C₁₀H₁₅O₄S^(1-); at 25 ℃; for 0.5h;

DOI:10.1016/j.molliq.2020.114370

Reference yield: 83.0%

morpholine (110-91-8,99108-56-2) + β-iodopropiophenone (24070-51-7) → 3-morpholin-4-yl-1-phenyl-propan-1-one (2298-48-8)

Guidance literature:

In tetrahydrofuran; for 4h; Inert atmosphere; Reflux;

DOI:10.1248/bpb.34.538

Reference yield: 75.0%

bromobenzene (108-86-1,52753-63-6) + N-methoxy-N-methyl-3-morpholinopropanamide (405212-49-9) → 3-morpholin-4-yl-1-phenyl-propan-1-one (2298-48-8)

Guidance literature:

bromobenzene; With magnesium; In tetrahydrofuran; for 1h; Heating;

N-methoxy-N-methyl-3-morpholinopropanamide; In tetrahydrofuran; at 0 ℃;

DOI:10.1055/s-2001-18439

upstream raw materials:

3-Morpholin-4-yl-propionitrile

formaldehyd

morpholinium hydrobromide

acetophenone

Downstream raw materials:

4-methyl-4-nitro-1-phenylpentan-1-one

3-Morpholino-1,1-diphenyl-1-propanol

1-phenyl-3-(2-oxocyclopentyl)-1-propanone

3-benzylsulfanyl-1-phenyl-1-propanone

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