1-methyl-cyclopropanecarboxylic acid benzoylamide

Base Information

• Chemical Name: 1-methyl-cyclopropanecarboxylic acid benzoylamide
• CAS No.: 1020077-90-0
• Molecular Formula: C₁₂H₁₃NO₂
• Molecular Weight: 203.241
• Mol file: 1020077-90-0.mol

Synonyms:1-methyl-cyclopropanecarboxylic acid benzoylamide

Chemical Property of 1-methyl-cyclopropanecarboxylic acid benzoylamide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-methyl-cyclopropanecarboxylic acid benzoylamide

There total 1 articles about 1-methyl-cyclopropanecarboxylic acid benzoylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1-methylcyclopropanecarbonyl chloride (16480-05-0) + benzamide (55-21-0,27208-38-4) → 1-methyl-cyclopropanecarboxylic acid benzoylamide (1020077-90-0)

Guidance literature:

benzamide; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

1-methylcyclopropanecarbonyl chloride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol800401g

Reference yield:

1-methyl-cyclopropanecarboxylic acid benzoylamide (1020077-90-0) → C12H13NO2 (144945-22-2)

Guidance literature:

With chloro-trimethyl-silane; benzaldehyde; lithium iodide; scandium tris(trifluoromethanesulfonate); In dichloromethane; at 0 ℃; for 48h; Inert atmosphere;

DOI:10.1021/ol800401g

Reference yield:

chloro-trimethyl-silane (75-77-4) + 1-methyl-cyclopropanecarboxylic acid benzoylamide (1020077-90-0) + cyclohexanecarbaldehyde (2043-61-0) → C22H33NO3Si

Guidance literature:

chloro-trimethyl-silane; 1-methyl-cyclopropanecarboxylic acid benzoylamide; cyclohexanecarbaldehyde; With sodium iodide; scandium tris(trifluoromethanesulfonate); In dichloromethane; at 0 ℃; for 48h; Inert atmosphere;

With triethylamine; In dichloromethane; at 0 - 25 ℃;

DOI:10.1021/ol800401g

upstream raw materials:

1-methylcyclopropanecarbonyl chloride

benzamide

Downstream raw materials:

C₁₂H₁₃NO₂