2,4,6,8-TETRAMETHYLQUINOLINE

Base Information

• Chemical Name: 2,4,6,8-TETRAMETHYLQUINOLINE
• CAS No.: 49616-71-9
• Molecular Formula: C₁₃H₁₅N
• Molecular Weight: 185.269
• Mol file: 49616-71-9.mol

Synonyms:2,4,6,8-Tetramethylquinoline

Chemical Property of 2,4,6,8-TETRAMETHYLQUINOLINE

Chemical Property:

• Vapor Pressure: 0.005mmHg at 25°C
• Refractive Index: 1.591
• Boiling Point: 284.499°C at 760 mmHg
• Flash Point: 124.321°C
• PSA: 12.89000
• Density: 1.019g/cm³
• LogP: 3.46840

Purity/Quality:

98%Min ^*data from raw suppliers

2,4,6,8-Tetramethylquinoline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6,8-TETRAMETHYLQUINOLINE

There total 6 articles about 2,4,6,8-TETRAMETHYLQUINOLINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dimethyl-6-(1'-methyl-2'-buten-1'-yl)aniline (109540-62-7) → 2,4,6,8-tetramethylquinoline (49616-71-9) + 2-Ethyl-3,5,7-trimethyl-1H-indole (98609-09-7)

Guidance literature:

With PdCl₂-(DMSO)n; In nitrobenzene; at 170 ℃; for 2h; Yield given. Yields of byproduct given; autoclave;

DOI:10.1007/BF00546739

Reference yield:

C13H17NO → 2,4,6,8-tetramethylquinoline (49616-71-9)

Guidance literature:

With sulfuric acid; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.7b00389

Reference yield:

acetone (67-64-1) + paracetaldehyde (123-63-7) → 2,4,6,8-tetramethylquinoline (49616-71-9)

Guidance literature:

DOI:10.1021/ja01456a039

upstream raw materials:

2,4-dimethyl-6-(1'-methyl-2'-buten-1'-yl)aniline

acetone

paracetaldehyde

acetylacetone

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