9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine

Base Information

Chemical Name:9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine
CAS No.:867259-42-5
Molecular Formula:C₂₈H₄₆N₆O₃Si₂
Molecular Weight:570.883
Hs Code.:

Synonyms:9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine

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Chemical Property of 9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine

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Technology Process of 9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine

There total 5 articles about 9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867259-40-3
2-amino-4-[3,5-bis(hydroxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

: 867259-42-5
9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / imidazole / dimethylformamide / 18 h / 20 °C

2: Zn; AcOH / H₂O; ethanol; tetrahydrofuran / 1 h / Heating

3: 3.70 g / dimethylformamide / 15 h / 20 °C

With 1H-imidazole; acetic acid; zinc; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo050635m

Reference yield:

: 867259-41-4
2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

: 867259-42-5
9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine

Guidance literature:: Multi-step reaction with 2 steps

1: Zn; AcOH / H₂O; ethanol; tetrahydrofuran / 1 h / Heating

2: 3.70 g / dimethylformamide / 15 h / 20 °C

With acetic acid; zinc; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo050635m

Reference yield:

: 71176-54-0
(3-amino-5-hydroxymethylphenyl)methanol

: 867259-42-5
9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]-2-N-[(dimethylamino)methylene]guanine

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / ethanol / 7 h / Heating

2: 99 percent / imidazole / dimethylformamide / 18 h / 20 °C

3: Zn; AcOH / H₂O; ethanol; tetrahydrofuran / 1 h / Heating

4: 3.70 g / dimethylformamide / 15 h / 20 °C

With 1H-imidazole; acetic acid; zinc; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo050635m