2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

Base Information

Chemical Name:2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine
CAS No.:867259-41-4
Molecular Formula:C₃₀H₄₆N₆O₃Si₂
Molecular Weight:594.905
Hs Code.:

Synonyms:2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

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Technology Process of 2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

There total 3 articles about 2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 867259-40-3
2-amino-4-[3,5-bis(hydroxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

: 18162-48-6
tert-butyldimethylsilyl chloride

: 867259-41-4
2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1021/jo050635m

Reference yield:

: 71176-54-0
(3-amino-5-hydroxymethylphenyl)methanol

: 867259-41-4
2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / ethanol / 7 h / Heating

2: 99 percent / imidazole / dimethylformamide / 18 h / 20 °C

With 1H-imidazole; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo050635m

Reference yield:

: 30412-45-4
2-amino-4-chloro-6-hydroxy-5-phenylazopyrimidine

: 867259-41-4
2-amino-4-[3,5-bis(tert-butyldimethylsilanyloxymethyl)anilino]-6-hydroxy-5-phenylazopyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / ethanol / 7 h / Heating

2: 99 percent / imidazole / dimethylformamide / 18 h / 20 °C

With 1H-imidazole; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo050635m