N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

Base Information

Chemical Name:N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate
CAS No.:1391631-80-3
Molecular Formula:C₅H₁₁NO*C₁₄H₁₄N₂O₂S
Molecular Weight:375.492
Hs Code.:

Synonyms:N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

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Technology Process of N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

There total 4 articles about N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-02-4
4-methyl-morpholine

: 2033-24-1
cycl-isopropylidene malonate

: 7357-70-2
Cyanothioacetamide

: 613-69-4
2-ethoxylbenzaldehyde

: 1391631-80-3
N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

Guidance literature:: In ethanol; Reflux;
DOI:10.1080/10426507.2016.1224877

Reference yield:

: 613-69-4
2-ethoxylbenzaldehyde

: 1391631-80-3
N-methylmorpholinium 3-cyano-4-(2-ethoxyphenyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 1 h / 20 °C

2: ethanol / Reflux

In ethanol;
DOI:10.1007/s10593-012-1016-0