(-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane

Base Information

Chemical Name:(-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane
CAS No.:334757-47-0
Molecular Formula:C₁₃H₁₉NO₂S
Molecular Weight:253.365
Hs Code.:

Synonyms:(-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane

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Technology Process of (-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane

There total 2 articles about (-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 334757-17-4
(-)-(S)-S-Phenylethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-thiocarboxylate

: 334757-47-0
(-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane

Guidance literature:: With methanesulfonic acid; In methanol; diethyl ether; for 72h; Heating;
DOI:10.1002/1521-3765(20010119)7:2<423::AID-CHEM423>3.0.CO;2-Y

Reference yield:

: 146176-60-5
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride

: 334757-47-0
(-)-(S)-S-1-[N-(2-Hydroxy-1,1-dimethylethyl)-aminocarbonylthio]-1-phenylethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 0.5 h / 20 °C

1.2: 97 percent / tetrahydrofuran / 3 h / Heating

2.1: 93 percent / MsOH / methanol; diethyl ether / 72 h / Heating

With methanesulfonic acid; sodium hydride; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/1521-3765(20010119)7:2<423::AID-CHEM423>3.0.CO;2-Y