N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Base Information

Chemical Name:N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene
CAS No.:304862-46-2
Molecular Formula:C₂₈H₃₉ClN₂O₄S₂
Molecular Weight:567.214
Hs Code.:

N<sup>3</sup>,N<sup>8</sup>-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Synonyms:N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Suppliers and Price of N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

There total 5 articles about N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1476-11-5
Z-1,4-dichlorobutene

: 304862-42-8
N¹,N⁴-bis(mesitylenesulfonyl)-N⁴-ethyl-1,4-diamino-2-butene

: 304862-46-2
N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Guidance literature:: N¹,N⁴-bis(mesitylenesulfonyl)-N⁴-ethyl-1,4-diamino-2-butene; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Z-1,4-dichlorobutene; In N,N-dimethyl-formamide; at 50 ℃; for 18h; Further stages.;
DOI:10.1021/jm000310s

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 304862-46-2
N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / aq. KOH / dioxane / 20 °C

2.1: NaH / dimethylformamide / 2 h / 20 °C

2.2: 97 percent / dimethylformamide / 18 h / 50 °C

With potassium hydroxide; sodium hydride; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm000310s

Reference yield:

: 151915-07-0
N-ethyl-(2-mesitylene)sulfonamide

: 304862-46-2
N³,N⁸-bis(mesitylenesulfonyl)-12-chloro-3,8-diaza-(5Z,10Z)-dodecadiene

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / dimethylformamide / 1 h / 20 °C

1.2: 82 percent / dimethylformamide / 18 h / 80 °C

2.1: 65 percent / H₂NNH₂ / methanol / 24 h / 55 °C

3.1: 96 percent / aq. KOH / dioxane / 20 °C

4.1: NaH / dimethylformamide / 2 h / 20 °C

4.2: 97 percent / dimethylformamide / 18 h / 50 °C

With potassium hydroxide; sodium hydride; hydrazine; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm000310s