Al₂(i-Bu)4

Base Information

Chemical Name:Al₂(i-Bu)4
CAS No.:60253-71-6
Molecular Formula:C₁₆H₃₆Al₂
Molecular Weight:282.425
Hs Code.:

Synonyms:Al₂(i-Bu)4

Suppliers and Price of Al₂(i-Bu)4

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Al₂(i-Bu)4

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Al₂(i-Bu)4

There total 1 articles about Al₂(i-Bu)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7440-09-7
potassium

: 1779-25-5
diisobutylaluminum chloride

: isobutyl potassium

: potassium triisobutyldialuminum

: 60253-71-6
Al₂(i-Bu)4

Guidance literature:: In Cyclopentane; i-Bu2AlCl dissolved in cyclopentane is slowly added to K slivers; reactants maintained at 0°C for 24 h followed by 48 h at ca. 25°C; cyclopentane added to the reaction mixt. followed by additional K; stirring for additional 2 d; filtration, cyclopentane affords KAl2(i-Bu)3 + Al2(i-Bu)4; elem. anal.;
DOI:10.1016/S0020-1693(00)86378-1

Reference yield:

: 7647-01-0,15364-23-5
hydrogenchloride

: 60253-71-6
Al₂(i-Bu)4

: 75-28-5,40921-86-6
Isobutane

: 1888-87-5
isobutylaluminum dichloride

: 1779-25-5
diisobutylaluminum chloride

Guidance literature:: In Cyclopentane; byproducts: H2; 2 h, 25°C; filtered, treated with H2O; identified by (1)H NMR;
DOI:10.1021/om00127a010

Reference yield:

: 60253-71-6
Al₂(i-Bu)4

: 100-99-2,130565-62-7
triisobutylaluminum

: 7429-90-5
aluminium

Guidance literature:: With trimethylaluminum; In Cyclopentane; byproducts: H2, CH4, isobutane; dissolving Al2((CH3)2CHCH2)4 in cyclopentane; cooling to -196°C;treating with Al(CH3)3; slow warming to room temperature; pptn. after 2h; stirring at 0°C for 10 h; filtn., Al was isolated as 8-hydroxyquinolate; Al((CH3)2CHCH2)3 was notisolated but decomposed after treating of the filtrate with H3O(1+);
DOI:10.1016/S0020-1693(00)82234-3