o-phenyl isopropyl ketone

Base Information

Chemical Name:o-phenyl isopropyl ketone
CAS No.:147531-54-2
Molecular Formula:C₂₄H₂₆NO₂P
Molecular Weight:391.45
Hs Code.:

o-<diphenylphosphinoylmethyl(methyl)amino>phenyl isopropyl ketone

Synonyms:o-phenyl isopropyl ketone

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Chemical Property of o-phenyl isopropyl ketone

Chemical Property:

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Technology Process of o-phenyl isopropyl ketone

There total 5 articles about o-phenyl isopropyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17583-40-3
2-methylaminobenzonitrile

: 147531-54-2
o-phenyl isopropyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) HCl / 1.) THF, Et₂O, 0 deg C, 5 h, 2.) H₂O, room temperature, 0.5 h

2: 1.) EtOH, 3.) K₂CO₃ / 1.) toluene, reflux, overnight, 2.) THF, room temperature, 1 h, 3.) 15 min

With hydrogenchloride; ethanol; potassium carbonate;
DOI:10.1039/P19930002463

Reference yield:

: 7505-81-9
2-methylaminobenzamide

: 147531-54-2
o-phenyl isopropyl ketone

Guidance literature:: Multi-step reaction with 4 steps

1: POCl₃ / pyridine

2: 2.) 10 percent HCl / 1.) Et₂O, a.) 0 deg C to r.t., b.) r.t., 5 h, 2.) 0 deg C, 3 h

3: toluene / Heating

4: 2.) K₂CO₃ / 1.) THF, r.t., 1 h, 2.) 15 min

With hydrogenchloride; potassium carbonate; trichlorophosphate; In pyridine; toluene;
DOI:10.1016/S0040-4020(01)90195-4

Reference yield:

: 32606-05-6
2-N-methylaminophenyl isopropyl ketone

: 147531-54-2
o-phenyl isopropyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / Heating

2: 2.) K₂CO₃ / 1.) THF, r.t., 1 h, 2.) 15 min

With potassium carbonate; In toluene;
DOI:10.1016/S0040-4020(01)90195-4