cyclopenta-2,4-dienyl-triphenyl stannane

Base Information

Chemical Name:cyclopenta-2,4-dienyl-triphenyl stannane
CAS No.:1238-38-6
Molecular Formula:C₂₃H₂₀Sn
Molecular Weight:415.122
Hs Code.:

Synonyms:cyclopenta-2,4-dienyl-triphenyl stannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclopenta-2,4-dienyl-triphenyl stannane

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Technology Process of cyclopenta-2,4-dienyl-triphenyl stannane

There total 4 articles about cyclopenta-2,4-dienyl-triphenyl stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 17306-10-4
cyclopentadienylmagnesium bromide

: 639-58-7
triphenyltin chloride

: 1238-38-6
cyclopenta-2,4-dienyl-triphenyl stannane

Guidance literature:: In diethyl ether; benzene; refluxing, 4 h;;
DOI:10.1021/jo01354a006

Reference yield: 71.3%

: 1092-86-0
dimethylamidotriphenyltin(IV)

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 1238-38-6
cyclopenta-2,4-dienyl-triphenyl stannane

Guidance literature:: In Petroleum ether; refluxing, 1 h;;
DOI:10.1016/S0022-328X(00)84649-5

Reference yield: 60.0%

: 894-09-7
iodotriphenylstannane

: cyclopentadienylthallium(I)

: thallium(I) iodide

: 1238-38-6
cyclopenta-2,4-dienyl-triphenyl stannane

Guidance literature:: In chloroform; under N2, dropwise addn. of a soln. of the Sn compound in CHCl3 to a soln. of the thallium compound in CHCl3 at room temp., stirring for 2 h, pptn. of TlI, filtration; concg. the soln., addn. of petroleum ether (60 - 80°), pptn., washing (petroleum ether), drying at 20°/10 mm Hg;