9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide

Base Information

• Chemical Name: 9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide
• CAS No.: 253439-77-9
• Molecular Formula: C₁₇H₂₀N₃O₂P
• Molecular Weight: 329.338

Synonyms:9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide

Chemical Property of 9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide

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Technology Process of 9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide

There total 1 articles about 9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide (183056-01-1) → 9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide (253439-77-9)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 5h;

DOI:10.1039/a904771i

Reference yield: 83.0%

benzyl bromide (100-39-0) + 9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide (253439-77-9) → 6-benzyl-9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide

Guidance literature:

9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

benzyl bromide; In tetrahydrofuran; hexane; at 20 ℃; for 20h;

DOI:10.1055/s-2000-6368

Reference yield: 78.0%

9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide (253439-77-9) + methyl iodide (74-88-4) → 9-methoxy-6-methyl-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide

Guidance literature:

9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

methyl iodide; In tetrahydrofuran; hexane; at 20 ℃; for 20h;

DOI:10.1055/s-2000-6368

upstream raw materials:

1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide

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