2-Ethynylbicyclo[2.2.1]heptan-2-ol

Base Information

Chemical Name:2-Ethynylbicyclo[2.2.1]heptan-2-ol
CAS No.:18084-03-2
Molecular Formula:C₉H₁₂O
Molecular Weight:136.194
Hs Code.:
European Community (EC) Number:826-930-4
Nikkaji Number:J754.891E

Synonyms:2-ethynylbicyclo[2.2.1]heptan-2-ol;18084-03-2;SCHEMBL5227729;DOBPSJXGDUDHTH-UHFFFAOYSA-N;AKOS020111666;EN300-380916;Z1460824343

Suppliers and Price of 2-Ethynylbicyclo[2.2.1]heptan-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Ethynylbicyclo[2.2.1]heptan-2-ol

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:136.088815002
Heavy Atom Count:10
Complexity:200

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C#CC1(CC2CCC1C2)O

Technology Process of 2-Ethynylbicyclo[2.2.1]heptan-2-ol

There total 4 articles about 2-Ethynylbicyclo[2.2.1]heptan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 497-38-1
Norbornan-2-on

: 18084-03-2,55373-77-8
2-exo-ethynylbicyclo<2.2.1>heptan-2-ol

Guidance literature:: In tetrahydrofuran; Ambient temperature;
DOI:10.1016/S0040-4020(01)89294-2

Reference yield: 82.0%

: 497-38-1
Norbornan-2-on

: 75-20-7
calcium carbide

: 18084-03-2,55373-77-8
2-exo-ethynylbicyclo<2.2.1>heptan-2-ol

Guidance literature:: With tetrabutyl ammonium fluoride; water; In dimethyl sulfoxide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/acs.orglett.5b01219

Reference yield:

: 497-38-1
Norbornan-2-on

: 1216963-74-4
lithium acetylide-ethylenediamine complex

: 18084-03-2
2-ethynylbicyclo[2.2.1]heptan-2-ol

Guidance literature:: Norbornan-2-on; lithium acetylide-ethylenediamine complex; In tetrahydrofuran; at 20 ℃; for 18h;

With water; In tetrahydrofuran;