6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Base Information

Chemical Name:6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone
CAS No.:80170-56-5
Molecular Formula:C₂₁H₂₀Cl₄N₂O
Molecular Weight:458.215
Hs Code.:

Synonyms:6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

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Technology Process of 6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

There total 4 articles about 6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 80170-45-2
syn-5-chloro-2-trichloracetamidobenzophenone cyclohexylimine

: 80170-56-5
6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; at 100 ℃; for 7h;
DOI:10.1248/cpb.29.2135

Reference yield: 8.0%

: 26381-66-8
5-chloro-2-trichloroacetylaminobenzophenone

: 108-91-8,157973-60-9
cyclohexylamine

: 25514-22-1
1-(2-benzoyl-4-chlorophenyl)-3-cyclohexylurea

: 719-59-5
5-chloro-2-aminobenzophenone

: 80170-81-6
6-chloro-3-cyclohexyl-3,4-dihydro-4-hydroxy-4-phenyl-2(1H)-quinazolinone

: 80170-56-5
6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; at 100 ℃; for 7h; Further byproducts given;
DOI:10.1248/cpb.29.2135

Reference yield:

: 26381-66-8
5-chloro-2-trichloroacetylaminobenzophenone

: 80170-56-5
6-chloro-3-cyclohexyl-3,4-dihydro-4-phenyl-4-trichloromethyl-2(1H)-quinazolinone

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / TiCl₄ / benzene / 4 h / Ambient temperature

2: 67 percent / hexamethylphosphoric acid triamide / 7 h / 100 °C

With titanium tetrachloride; In N,N,N,N,N,N-hexamethylphosphoric triamide; benzene;
DOI:10.1248/cpb.29.2135