Technology Process of C15H21NO2
There total 6 articles about C15H21NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.1021/ol070415q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 0.44 g / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C
2: Dess-Martin periodinane / CH2Cl2 / 20 °C
3: 0.68 g / 2-methyl-2-butene; sodium chlorite; sodium dihydrogen phosphate monohydrate / 2-methyl-propan-2-ol; H2O; tetrahydrofuran / 20 °C
4: 0.36 g / cesium carbonate / dimethylformamide
5: 100 percent / trifluoroacetic acid / CH2Cl2 / 2 h / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; caesium carbonate; Dess-Martin periodane; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol070415q
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Dess-Martin periodinane / CH2Cl2 / 20 °C
2: 0.68 g / 2-methyl-2-butene; sodium chlorite; sodium dihydrogen phosphate monohydrate / 2-methyl-propan-2-ol; H2O; tetrahydrofuran / 20 °C
3: 0.36 g / cesium carbonate / dimethylformamide
4: 100 percent / trifluoroacetic acid / CH2Cl2 / 2 h / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; caesium carbonate; Dess-Martin periodane; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ol070415q
