3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine

Base Information

Chemical Name:3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine
CAS No.:1616634-99-1
Molecular Formula:C₁₄H₁₁BBrN
Molecular Weight:283.963
Hs Code.:

Synonyms:3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine

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Technology Process of 3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine

There total 3 articles about 3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24341-84-2
2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine

: 1616634-99-1
3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine

Guidance literature:: With bromine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo5011894

Reference yield:

: 3867-18-3
2-vinylaniline

: 1616634-99-1
3-bromo-2-phenyl-1,2-dihydrobenzo[e][1,2]azaborinine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrachlorosilane; triethylamine / toluene / 16 h / 40 °C / Sealed tube; Inert atmosphere

2: bromine / dichloromethane / 2 h / 0 - 20 °C / Sealed tube

With tetrachlorosilane; bromine; triethylamine; In dichloromethane; toluene;
DOI:10.1021/acs.orglett.6b00466