ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate

Base Information

Chemical Name:ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate
CAS No.:118970-26-6
Molecular Formula:C₃₆H₃₇NO₁₂
Molecular Weight:675.689
Hs Code.:

Synonyms:ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate

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Chemical Property of ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate

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Technology Process of ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate

There total 2 articles about ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 118970-25-5,119066-42-1
ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylcarbamate

: 118970-26-6
ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate

Guidance literature:: With ammonium bromide; at 20 - 25 ℃; for 0.833333h; electrolyzed under current of 0.01 amp at 14V;
DOI:10.1002/jhet.5570250227

Reference yield:

: 86528-49-6
2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)furan

: 118970-26-6
ethyl 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,5-dimethoxy-2,5-dihydro-2-furfurylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 100 percent / ammonium bromide / 0.83 h / 20 - 25 °C / electrolyzed under current of 0.01 amp at 14V

With ammonium bromide; toluene-4-sulfonic acid; In benzene;
DOI:10.1002/jhet.5570250227