C₂₂H₁₉ClO₄

Base Information

Chemical Name:C₂₂H₁₉ClO₄
CAS No.:1254352-28-7
Molecular Formula:C₂₂H₁₉ClO₄
Molecular Weight:382.843
Hs Code.:

C<sub>22</sub>H<sub>19</sub>ClO<sub>4</sub>

Synonyms:C₂₂H₁₉ClO₄

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Chemical Property of C₂₂H₁₉ClO₄

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Technology Process of C₂₂H₁₉ClO₄

There total 12 articles about C₂₂H₁₉ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1254340-88-9
phenyl 6-(benzyloxy)-3-chloro-4-formyl-2-methylbenzoate

: 1254352-28-7
C₂₂H₁₉ClO₄

Guidance literature:: With methanol; sodium tetrahydroborate;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1254352-28-7
C₂₂H₁₉ClO₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5.1: N-chloro-succinimide / acetonitrile / 45 h / 60 °C

6.1: boron tribromide / dichloromethane / 0.75 h / -78 - 0 °C

6.2: 0.17 h / 20 °C

7.1: potassium carbonate / acetone / 20 °C

8.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1.17 h / -78 - 0 °C / Inert atmosphere

8.2: 0.5 h / 20 °C

9.1: sodium tetrahydroborate; methanol

With methanol; dmap; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; N-chloro-succinimide; 2-methyl-but-2-ene; oxalyl dichloride; water; isopropylmagnesium chloride; boron tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; lithium chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetone; toluene; acetonitrile; tert-butyl alcohol;

Reference yield:

: 877149-08-1
4-bromo-2-methoxy-6-methyl-benzoic acid

: 1254352-28-7
C₂₂H₁₉ClO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

3.1: N-chloro-succinimide / acetonitrile / 45 h / 60 °C

4.1: boron tribromide / dichloromethane / 0.75 h / -78 - 0 °C

4.2: 0.17 h / 20 °C

5.1: potassium carbonate / acetone / 20 °C

6.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1.17 h / -78 - 0 °C / Inert atmosphere

6.2: 0.5 h / 20 °C

7.1: sodium tetrahydroborate; methanol

With methanol; dmap; sodium tetrahydroborate; N-chloro-succinimide; oxalyl dichloride; isopropylmagnesium chloride; boron tribromide; potassium carbonate; triethylamine; lithium chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;