5-BROMO-3-(BROMOMETHYL)PYRIDIN-2-AMINE HYDROBROMIDE

Base Information

• Chemical Name: 5-BROMO-3-(BROMOMETHYL)PYRIDIN-2-AMINE HYDROBROMIDE
• CAS No.: 335033-38-0
• Molecular Formula: BrH*C₆H₆Br₂N₂
• Molecular Weight: 346.847
• Mol file: 335033-38-0.mol

Synonyms:2-Pyridinamine,5-bromo-3-(bromomethyl)-, monohydrobromide (9CI); (5-Bromo-3-bromomethylpyridin-2-yl)aminehydrobromide; 2-Amino-5-bromo-3-(bromomethyl)pyridine hydrobromide

Chemical Property of 5-BROMO-3-(BROMOMETHYL)PYRIDIN-2-AMINE HYDROBROMIDE

Chemical Property:

• PSA: 38.91000
• LogP: 3.86050
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-Bromo-3-(bromomethyl)pyridin-2-aminehydrobromide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-BROMO-3-(BROMOMETHYL)PYRIDIN-2-AMINE HYDROBROMIDE

There total 5 articles about 5-BROMO-3-(BROMOMETHYL)PYRIDIN-2-AMINE HYDROBROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-amino-5-bromo-3-(hydroxymethyl)pyridine (335031-01-1) → 2-amino-5-bromo-3-(bromomethyl)pyridine hydrobromide (335033-38-0)

Guidance literature:

With hydrogen bromide; In water; Product distribution / selectivity; Reflux;

Reference yield: 84.0%

(2-amino-5-bromopyridine-3-yl)methanol hydrobromide (443956-55-6) → 2-amino-5-bromo-3-(bromomethyl)pyridine hydrobromide (335033-38-0)

Guidance literature:

With hydrogen bromide; for 10h; Reflux; Inert atmosphere;

Reference yield: 58.0%

malonic acid dimethyl ester (108-59-8) → 6-bromo-2-oxo-1,2,3,4-tetrahydro-1,8-naphthyridine-3-carboxylic acid methyl ester (335031-10-2) + 2-amino-5-bromo-3-(bromomethyl)pyridine hydrobromide (335033-38-0)

Guidance literature:

With sodium methylate; In methanol;

upstream raw materials:

2-amino-5-bromo-3-(hydroxymethyl)pyridine

(2-amino-3-pyridinyl)methanol

malonic acid dimethyl ester

2-aminopyridin-3-carboxylic acid

Downstream raw materials:

6-bromo-2-oxo-1,2,3,4-tetrahydro-1,8-naphthyridine-3-carboxylic acid methyl ester

tert-butyl 6-bromo-2-oxo-2,4-dihydro-1H-spiro[[1,8]naphthyridine-3,4'-piperidine]-1'-carboxylate

7-bromo-1,3,4,5-tetrahydro-pyrido[2,3-e][1,4]diazepin-2-one

tert-butyl 7-bromo-2-oxo-2,3-dihydro-1H-pyrido[2,3-e][1,4]diazepine-4(5H)-carboxylate

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