benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether

Base Information

Chemical Name:benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether
CAS No.:220489-26-9
Molecular Formula:C₂₂H₃₀O
Molecular Weight:310.48
Hs Code.:

Synonyms:benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether

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Chemical Property of benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether

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Technology Process of benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether

There total 8 articles about benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 220489-26-9
benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium hydride / 1.) DMF, 2.) DMF, 1 h

2: 85 percent / tin(IV) chloride / CH₂Cl₂ / 3 h / -50 - -15 °C

4: 78 percent / potassium hydroxide / methanol; H₂O / 6 h / 120 °C

5: 1.) NaCH₂SOCH₃ / 1.) DMSO, mineral oil, 15 min, 2.) DMSO, mineral oil, room temperature, 30 min

With potassium hydroxide; tin(IV) chloride; sodium hydride; sodium methylsulfinylmethanide; In methanol; dichloromethane; water;
DOI:10.1021/jo982020d

Reference yield:

: 88794-46-1
(-)-2,2,6-trimethyl-7-oxabicyclo[4.1.0]heptane-1-methanol

: 220489-26-9
benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium hydride / 1.) DMF, 2.) DMF, 1 h

2: 85 percent / tin(IV) chloride / CH₂Cl₂ / 3 h / -50 - -15 °C

4: 78 percent / potassium hydroxide / methanol; H₂O / 6 h / 120 °C

5: 1.) NaCH₂SOCH₃ / 1.) DMSO, mineral oil, 15 min, 2.) DMSO, mineral oil, room temperature, 30 min

With potassium hydroxide; tin(IV) chloride; sodium hydride; sodium methylsulfinylmethanide; In methanol; dichloromethane; water;
DOI:10.1021/jo982020d

Reference yield:

: 220489-20-3
2-benzyloxy-1-<(1S)-1,2,2-trimethylcyclopentyl>-1-ethanone

: 220489-26-9
benzyl 4-methylene-2-<(1S)-1,2,2-trimethylcyclopentyl>-2-cyclohexenyl-ether

Guidance literature:: Multi-step reaction with 3 steps

2: 78 percent / potassium hydroxide / methanol; H₂O / 6 h / 120 °C

3: 1.) NaCH₂SOCH₃ / 1.) DMSO, mineral oil, 15 min, 2.) DMSO, mineral oil, room temperature, 30 min

With potassium hydroxide; sodium methylsulfinylmethanide; In methanol; water;
DOI:10.1021/jo982020d