p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Base Information

Chemical Name:p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside
CAS No.:359686-41-2
Molecular Formula:C₃₀H₃₄O₁₂
Molecular Weight:586.593
Hs Code.:

Synonyms:p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Suppliers and Price of p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

There total 3 articles about p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 31770-76-0
3-(4-hydroxyphenyl)propionic acid benzyl ester

: 4163-60-4
β-D-galactose peracetate

: 359686-41-2
p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -19 ℃; for 1h;
DOI:10.1081/CAR-100103953

Reference yield:

: 501-97-3
4-hydroxyphenylpropionic acid

: 359686-41-2
p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 765 mg / KHCO₃ / dimethylformamide / 12 h / 20 °C

2: 59 percent / SnCl₄ / CH₂Cl₂ / 1 h / -19 °C

With tin(IV) chloride; potassium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-100103953

Reference yield:

: 100-39-0
benzyl bromide

: 359686-41-2
p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 765 mg / KHCO₃ / dimethylformamide / 12 h / 20 °C

2: 59 percent / SnCl₄ / CH₂Cl₂ / 1 h / -19 °C

With tin(IV) chloride; potassium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-100103953