5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

Base Information

Chemical Name:5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine
CAS No.:1433363-10-0
Molecular Formula:C₁₆H₁₈ClN₅O
Molecular Weight:331.805
Hs Code.:

Synonyms:5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

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Chemical Property of 5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

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Technology Process of 5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

There total 7 articles about 5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1433362-88-9
5-tert-butyl-3-(4-methoxybenzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-7(4H)-one

: 1433363-10-0
5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

Guidance literature:: With trichlorophosphate; In N,N-dimethyl-aniline; for 4h; Inert atmosphere; Reflux;

Reference yield:

: 133992-53-7
5-amino-1-[(4-methoxyphenyl)methyl]-1,2,3-triazole-4-carboxamide

: 1433363-10-0
5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 2 h / 80 °C / Inert atmosphere

1.2: 1 h / 80 °C / Inert atmosphere

1.3: 18 h / Reflux

2.1: N,N-diethylaniline; trichlorophosphate / 4 h / Reflux; Inert atmosphere

With pyridine; N,N-diethylaniline; trichlorophosphate;

Reference yield:

: 70978-37-9
1-(azidomethyl)-4-methoxybenzene

: 1433363-10-0
5-tert-butyl-7-chloro-3-(4-methoxy benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium ethanolate / ethanol / 21 h / Inert atmosphere; Reflux

2.1: pyridine / 2 h / 80 °C / Inert atmosphere

2.2: 1 h / 80 °C / Inert atmosphere

2.3: 18 h / Reflux

3.1: N,N-diethylaniline; trichlorophosphate / 4 h / Reflux; Inert atmosphere

With pyridine; sodium ethanolate; N,N-diethylaniline; trichlorophosphate; In ethanol;