2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate

Base Information

Chemical Name:2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate
CAS No.:1363375-69-2
Molecular Formula:C₂₃H₂₆FNO₆S₂
Molecular Weight:495.593
Hs Code.:

Synonyms:2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate

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Chemical Property of 2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate

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Technology Process of 2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate

There total 5 articles about 2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1363375-69-2
2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate

Guidance literature:

Reference yield: 78.0%

: 1363375-23-8
2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethanol

: 124-63-0
methanesulfonyl chloride

: 1363375-69-2
2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jm301370e

Reference yield:

: 1363375-70-5
1-(4-fluorophenyl)-2-methyl-5-(4-(methylsulfonyl)phenyl)-3-(2-((tetrahydro-2H-pyran-2-yloxy)ethoxy)ethyl)-1H-pyrrole

: 1363375-69-2
2-[2-[2-(1-(4-fluorophenyl)-2-methyl-5-(4-methylsulphonylphenyl)-1H-pyrrol-3-yl)]ethoxy]ethyl methanesulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / methanol / 1 h / 55 °C

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C

With dmap; pyridinium p-toluenesulfonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/jm301370e