2,6-bis(3-bromopropyl)anisole

Base Information

Chemical Name:2,6-bis(3-bromopropyl)anisole
CAS No.:1361411-89-3
Molecular Formula:C₁₃H₁₈Br₂O
Molecular Weight:350.093
Hs Code.:

Synonyms:2,6-bis(3-bromopropyl)anisole

Suppliers and Price of 2,6-bis(3-bromopropyl)anisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,6-bis(3-bromopropyl)anisole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,6-bis(3-bromopropyl)anisole

There total 6 articles about 2,6-bis(3-bromopropyl)anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.3%

: 360556-72-5
3-[3-(3-hydroxypropyl)-2-methoxyphenyl]propanol

: 1361411-89-3
2,6-bis(3-bromopropyl)anisole

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.tet.2012.02.014

Reference yield:

: 3382-99-8
2,6-diallylphenol

: 1361411-89-3
2,6-bis(3-bromopropyl)anisole

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; sodium iodide / acetone / 48 h / 45 °C / Inert atmosphere

2.1: borane-THF / tetrahydrofuran / 3.5 h / -10 - 20 °C / Inert atmosphere

2.2: 3 h / 20 - 40 °C / Inert atmosphere

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 24 h / 0 - 20 °C

With borane-THF; carbon tetrabromide; potassium carbonate; triphenylphosphine; sodium iodide; In tetrahydrofuran; dichloromethane; acetone; 1.1: Williamson synthesis;
DOI:10.1016/j.tet.2012.02.014

Reference yield:

: 1746-13-0
allyl phenyl ether

: 1361411-89-3
2,6-bis(3-bromopropyl)anisole

Guidance literature:: Multi-step reaction with 6 steps

1.1: 200 - 205 °C / Neat (no solvent)

2.1: potassium carbonate; sodium iodide / acetone / 45 °C

3.1: 200 - 205 °C / Neat (no solvent)

4.1: potassium carbonate; sodium iodide / acetone / 48 h / 45 °C / Inert atmosphere

5.1: borane-THF / tetrahydrofuran / 3.5 h / -10 - 20 °C / Inert atmosphere

5.2: 3 h / 20 - 40 °C / Inert atmosphere

6.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 24 h / 0 - 20 °C

With borane-THF; carbon tetrabromide; potassium carbonate; triphenylphosphine; sodium iodide; In tetrahydrofuran; dichloromethane; acetone; 1.1: Claisen rearrangement / 2.1: Williamson synthesis / 3.1: Claisen rearrangement / 4.1: Williamson synthesis;
DOI:10.1016/j.tet.2012.02.014