1-(Allyloxy)-2-allylbenzene

Base Information

• Chemical Name: 1-(Allyloxy)-2-allylbenzene
• CAS No.: 3383-05-9
• Molecular Formula: C12H14O
• Molecular Weight: 174.243
• Hs Code.: 2909309090
• European Community (EC) Number: 682-396-0
• DSSTox Substance ID: DTXSID80448007
• Nikkaji Number: J522.147A
• Wikidata: Q82266922
• Mol file: 3383-05-9.mol

Synonyms:1-(Allyloxy)-2-allylbenzene;1-prop-2-enoxy-2-prop-2-enylbenzene;3383-05-9;o,o'-diallylphenol;AGN-PC-0NCNXB;SCHEMBL5085750;DTXSID80448007

Chemical Property of 1-(Allyloxy)-2-allylbenzene

Chemical Property:

• PSA: 9.23000
• LogP: 2.97990
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 174.104465066
• Heavy Atom Count: 13
• Complexity: 163

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C=CCC1=CC=CC=C1OCC=C

Technology Process of 1-(Allyloxy)-2-allylbenzene

There total 13 articles about 1-(Allyloxy)-2-allylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Allyl acetate (591-87-7) + o-Allylphenol (1745-81-9) → allyl 2-allylphenyl ether (3383-05-9)

Guidance literature:

With 5%-palladium/activated carbon; potassium carbonate; triphenylphosphine; In water; at 85 - 105 ℃; for 16h; Inert atmosphere;

Reference yield: 84.0%

allyl bromide (106-95-6) + o-Allylphenol (1745-81-9) → allyl 2-allylphenyl ether (3383-05-9)

Guidance literature:

With potassium carbonate; In acetone; for 1h; Reflux;

DOI:10.1002/hlca.202000216

Reference yield: 77.0%

allyl bromide (106-95-6) + o-(prop-2-enyloxy)phenylboronic acid (151414-76-5) → allyl 2-allylphenyl ether (3383-05-9)

Guidance literature:

With dichloro(N-(diphenylphosphino)-N-isopropyl-1,1-diphenylphosphinamine) digold(I); caesium carbonate; In acetonitrile; at 65 ℃; for 18h; chemoselective reaction;

DOI:10.1002/anie.201402924

upstream raw materials:

allyl bromide

o-Allylphenol

3-chloroprop-1-ene

phenol

Downstream raw materials:

2,6-diallylphenol

2,6-bis(3-bromopropyl)anisole

3,5-bis(3-bromopropyl)-4-methoxybenzaldehyde

4-(2-nitrovinyl)-2,6-bis(3-bromopropyl)anisole