C₁₄H₁₅F₂NO₅

Base Information

Chemical Name:C₁₄H₁₅F₂NO₅
CAS No.:1027927-06-5
Molecular Formula:C₁₄H₁₅F₂NO₅
Molecular Weight:315.274
Hs Code.:

C<sub>14</sub>H<sub>15</sub>F<sub>2</sub>NO<sub>5</sub>

Synonyms:C₁₄H₁₅F₂NO₅

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Chemical Property of C₁₄H₁₅F₂NO₅

Chemical Property:

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Technology Process of C₁₄H₁₅F₂NO₅

There total 8 articles about C₁₄H₁₅F₂NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 437-81-0
2,6-difluorobenzaldehyde

: 1027927-06-5
C₁₄H₁₅F₂NO₅

Guidance literature:: Multi-step reaction with 8 steps

1: triethylorthoformate, p-TSA / 1,2-dichloro-ethane / 2 h / 80 °C

2: 1.) n-BuLi / 1.) THF, -70 deg C, 20 min, 2.) THF, from -70 deg C to RT

3: SOCl₂, N,N-diisopropylamine / CH₂Cl₂ / 0 - 20 °C

4: CH₂Cl₂ / 0.5 h

5: p-TSA / H₂O; dioxane / 2 h / 60 °C

6: toluene / 0.5 h / 50 °C

7: H₂ / 10percent Pd/C / methanol; acetic acid / 1 h / 51.7 Torr

8: Et₃N

With n-butyllithium; thionyl chloride; hydrogen; toluene-4-sulfonic acid; triethylamine; diisopropylamine; orthoformic acid triethyl ester; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; water; acetic acid; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jm950639r

Reference yield:

: 1026500-48-0
2,4-Difluoro-3-formyl-N-methyl-benzamide

: 1027927-06-5
C₁₄H₁₅F₂NO₅

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 0.5 h / 50 °C

2: H₂ / 10percent Pd/C / methanol; acetic acid / 1 h / 51.7 Torr

3: Et₃N

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; acetic acid; toluene;
DOI:10.1021/jm950639r

Reference yield:

: 467442-18-8
2-(2,6-Difluoro-phenyl)-[1,3]dioxolane

: 1027927-06-5
C₁₄H₁₅F₂NO₅

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) n-BuLi / 1.) THF, -70 deg C, 20 min, 2.) THF, from -70 deg C to RT

2: SOCl₂, N,N-diisopropylamine / CH₂Cl₂ / 0 - 20 °C

3: CH₂Cl₂ / 0.5 h

4: p-TSA / H₂O; dioxane / 2 h / 60 °C

5: toluene / 0.5 h / 50 °C

6: H₂ / 10percent Pd/C / methanol; acetic acid / 1 h / 51.7 Torr

7: Et₃N

With n-butyllithium; thionyl chloride; hydrogen; toluene-4-sulfonic acid; triethylamine; diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; water; acetic acid; toluene;
DOI:10.1021/jm950639r